Volume 28 Issue 2

Published: 2019-06-01

Contents


Article
The Impact of Obesity on Infertile Women with Polycystic Ovaries in Iraq

Farah Kh. Al-Taie, Zena A. Al-Jawadi

The study has focused on obesityin women with Polycystic Ovary Syndrome (PCOS), as a potential new indicator of infertility by evaluating twelve biochemical and hormonal variables such...

DOI: 10.33899/rjs.2019.159964

Pages: 1-9
Clinical Study of Rhodanese Enzyme in Renal Failure Patients

Thikra A. Allwsh, Nawal Th. Younis, Rana F. Jasem

The research involved clinical study of rhodanese enzyme and its relation with some biochemical parameters in renal failure. The result demonstrated a significant increase in the activity of...

DOI: 10.33899/rjs.2019.159962

Pages: 1-7
Assessing the Environmental Situation for Excretion Management Stations in Al – Qayyarah Refinery

Yusra M. AL-Shaker, Amina B. Mohammed

The study was accomplished for the evaluation of the efficiency of the processing station of excretion in Al Qayyarah refinery, which is located in the area of Al Qayyarah town toward the south...

DOI: 10.33899/rjs.2019.159963

Pages: 8-22
Synthesis, Characterization and Antibacterial Activities of New Metal Complexes of Unsymmetrical Tetradentate Schiff Bases

Hussain I. Arteen, Hussain F. Hassan, Balsam K. Al-Fahhady, Israa M. Al-Nidaa, Khnsaa Sh. Al-Nama

Unsymmetrical Schiff baseH2L1=2-((8-((E)-1-((2-hydroxy phenyl) ethylidene amino) naphthalen-1-ylimino) methyl)-6-methoxyphenol and H2L2=1-((E)-(8-((E)-1-(2-hydroxy phenol) ethylidene amino)...

DOI: 10.33899/rjs.2019.159976

Pages: 10-22
Preparation, Characterization and Biological Activities of some Unsymmetrical Schiff Bases Derived from m-phenyelenediamine and their Metal Complexes

Rasha N. AL-Sadoon, Amera M. AL-Rawi, Moza M. Al- Jiboury, Khansaa Sh. Al- Nama

Unsymmetrical Schiff bases H2L1 = [ 1- (( E )-(( 3-((( E) -2- hydroxybenzylidene) amino)phenyl)imino)methyl) naphthalene-2-ol] and H2L2 = [1-((E)-((3-(((E)-1-(2-hydroxphenyl) ethylidene ) amino )...

DOI: 10.33899/rjs.2019.159965

Pages: 23-36
Synthesis and Biological Activity of some New Nitrogenous Heterocyclic Compounds Derived from Azachalcone

Hamad J. Jumaa, Munera Y. Roof, Shakir M. Saied

A series of heterocyclic compounds containing oxygen and nitrogen atoms, isoxazoline I(a-d) and another containing two nitrogen atoms, pyrazolinesII(a-d) and phenylpyrazolines IV(a-d) were prepared...

DOI: 10.33899/rjs.2019.159977

Pages: 37-46
Spectrophotometric Determination of Mesalazine in Pharmaceutical Preparations by Diazotization and Coupling with 2,6- Dihydroxytoluene as a New Coupling Agent

Manal A. Abd AL-Hayale, Najeeb K. Yousif, Alaa T. Aziz, Saad H. Sultan

A simple and sensitive spectrophotometric method is proposed for the determination of mesalazine (MZ) in some of its pharmaceutical preparations. The method is based on the diazotization of...

DOI: 10.33899/rjs.2019.159966

Pages: 47-55
Using of 2,7-Dihydroxynaphthalene as a Novel Reagent in Spectrophotometric Assay of Chloramphenicol

Nabeel S. Othman, Sudad R. Jamal

An indirect spectrophotometric method for the determination of chloramphenicol (CAP) has been suggested. The method is based on the oxidative coupling reaction of reduced chloramphenicol (R-CAP)...

DOI: 10.33899/rjs.2019.159978

Pages: 56-63
Electrochemical Behavior of Valsartan, Glibenclamide and their Interaction with Each other Using Square Wave Voltammetry

Amera M. Al-Rawi, Yousra Y. Agha, Aws Z. Al-Hafidh, Amer Th. Al-Taee

In this work an electrochemical behavior quantification and interaction of valsartan and glibenclamide were studied using square wave voltammetric technique. The effect of temperature on the...

DOI: 10.33899/rjs.2019.159967

Pages: 64-75
Spectrophotometric Determination of Paracetamol Using Diazotization Coupling Reaction

Enas S. Thanoon

An accurate, simple, and sensitive indirect spectrophotometric method which proposed and developed for the determination of paracetamol in different pharmaceutical preparations. The proposed method...

DOI: 10.33899/rjs.2019.159979

Pages: 76-83
Indirect Colorimetric Estimation of Fluoride Ion in Water and Pharmaceutical Preparation Samples

Nief R. Ahmad, Farha K. Omar

An indirect method for the estimation of fluoride ion has been developed.The method is based on the bleaching action of fluoride ion on the color of Ti (IV)with...

DOI: 10.33899/rjs.2019.159968

Pages: 84-89
Synthesis of Schiff Bases Derivatives from Benzene Diamine Containing Acridine Moiety

Sarab D. Sulyman, Shaimaa Y. Ibraheem, Rafid K. Jameel

One side of (o, m and p) benzene diamine reacted with aromatic aldehyde to give Schiff bases (Ia-d) or (IIa-d) and (IIIa-d) respectively. The second amine group of the synthesized Schiff bases...

DOI: 10.33899/rjs.2019.159980

Pages: 90-99
New Tridentate Hydrazone Metal Complexes Derived from 2-Hydroxy-4-Methoxyacetophenone and some Acid Hydrazides: Synthesis, Characterization and Antibacterial Activity Evaluation

Dhufr A. Omer, Abdul Ghany M. Al-Daher

A new series of complexes of Co(II), Ni(II), Cu(II), and Zn(II) with three hydrazones ligands(L) derived from 2-hydroxy-4-methoxy acetophenone (Paeonol) and 4-methylbenzoylhydrazide (AMBH), acetyl...

DOI: 10.33899/rjs.2019.159969

Pages: 100-111
Synthesis and Characterization of New Co(II), Ni(II), Cu(II) and Zn(II) with Bis-hydrazones Complexes

Ahmed A. Aldabagh, Abdul Ghany M. Al-Daher

A number of new Co(II), Ni(II), Cu(II) and Zn(II) complexes with 2,5-hexanedione bis(4-methylbenzoyl hydrazone)(HDMBH), 2,5-hexanedione bis(2-theonyl hydrazone)(HDTH) and 2,5-hexanedione...

DOI: 10.33899/rjs.2019.159981

Pages: 112-119
Electrochemical Study of Theophylline - Urea Interaction Using Square Wave Voltammetry

Asmaa M. Al-Hasany, Haitham A. Al-Wahb, Amer Th. Al-Taee

In this work, the interaction between theophylline (TP) which gives a stable well-defined reduction peak at (1.07) V versus Ag/AgCl. Sat. KCl/ in phosphate buffer solution (pH=7) and urea was...

DOI: 10.33899/rjs.2019.159970

Pages: 120-126
Spectrophotometric Determination of Mesalazine

Safaa A. Al-Zakaria

Mesalazine (MESA) is determined by a simple and rapid visible spectrophotometric method. This method is depend on oxidative coupling reaction of mesalazine with histidine (HIS) in alkaline media...

DOI: 10.33899/rjs.2019.159982

Pages: 127-134
Synthesis and Characterization of Some Novel Hydrazones of N-{11H-pyrido[2,1-b]quinazolin-11-one-9-yl} hydrazine

Attallah M. Sheat, Rafid K. Jameel

The 2-[(6-chloro-2-pyridyl) amino]benzoic acid (I) was synthesized viaUllmann-Goldberg coupling by reaction of anthranilic acid with2,6-dichloropyridine. The compound (I) was cyclized by using poly...

DOI: 10.33899/rjs.2019.159971

Pages: 135-145
Spectrophotometric Estimation of Thiamine in Tablet form Application to Content Uniformity Testing

Nief R. Ahmad, Wael A. Al-Qazzaz

A simple, rapid, accurate and sensitive spectrophotometric method for the determination of thiamine has been developed. The method is based on the direct reaction between thiamine and sodium...

DOI: 10.33899/rjs.2019.159983

Pages: 146-151
Electrochemical Biosensor Hemoglobin Immobilization Determination of the Breast Cancer Drug (Adriamycin)

Eman A. Al-Jawadi, Mohammed I. Majeed

Electrochemical biosensor is an effective tool for pharmaceutical analysis due to its simplicity, specificity, sensitivity, fast, cost effective and repetitive measurements with miniaturized and...

DOI: 10.33899/rjs.2019.159972

Pages: 152-163
Storage Stabilityand Compatibility of Dura Asphalt Modified by SBS

Doha N. Saad, Eman I. Ahmed

The purpose of this study was to characterize the physical behaviour of Dura asphalt modified by styrene-butadiene-styrene (SBS)co-polymer. The polymer modified asphalt (PMA) was produced by mixing...

DOI: 10.33899/rjs.2019.159984

Pages: 164-174
Square Wave Voltammetric and Computational Study of Thyroxine-Thiourea Interaction

Marwa N. Abdul-Fattah, Saddalah T. Sulaiman, Haitham A. AL-Wahab

The voltammetric behavior of Thyroxine (T4) was studied using square wave voltammetry in phosphate buffer solution at (pH 7.0) as supporting electrolyte. Thyroxine gives two well-defined reduction...

DOI: 10.33899/rjs.2019.159973

Pages: 175-183
Square Wave Voltammetric and Computational Study of the Thyroxine-Uracil Interaction

Marwa N. Abdul-Fattah, Saddalah T. Sulaiman, Haitham A. AL-Wahab

The voltammetric behavior of Thyroxine (T4) was studied using square wave voltammetry in phosphate buffer solution at (pH 7.0) as supporting electrolyte. Thyroxine gives two well-defined reduction...

DOI: 10.33899/rjs.2019.159985

Pages: 184-192
Interactions Study of Co-enzyme-Q0 with Aniline and Pyrrole Using Square Wave Voltammetric Technique

Nada B. Sharif, Saddalah T. Sulaiman, Kasim Y. Rahawi

The interactions of Co-enzyme Q0 with Aniline and Pyrrole were studied in aqueous phosphate buffer solution at (pH=7.0) as supporting electrolyte using square wave voltammetry, Co-enzyme Q0 gives a...

DOI: 10.33899/rjs.2019.159974

Pages: 193-203
Preparation and Physico Chemical Investigation of Manganese (II) Complexes with Hydrazone Ligands

Sahbaa A. Ahmed, Amira J. Al-Shaheen

The work reported deals with the preparation and characterization of a number of new complexes of manganese (II). The complexes are formed by the reaction of the mentioned metal salts with three...

DOI: 10.33899/rjs.2019.159986

Pages: 204-210
Studies on Preparation and Characterization of Blend Polymers for Hydrogels Synthesis and Use for Protein Release

Fawzi H. Jabrail, Rouaa K. Al-Ojar

Carboxy methyl cellulose, pectin, chitosan or acrylic acid poly (vinyl alcohol) blend hydrogels were prepared using Glutaraldehyde (GLU) as chemical or sodium hexameta phosphate (SHMP) as physical...

DOI: 10.33899/rjs.2019.159975

Pages: 211-227
Preparation and Characterization of some Transition Metal Complexes with OleylXanthate and 1,10- Phenanthrolin

Fayhaa K. AL-Jarah, Saad E. AL-Mukhtar

Xanthatecomplexes of the general formula [M{Ag(oleylXant)2}2] (A) and [MM'(oleylXant)4] (B) were M = Copper (II), Nickel II), Cobalt (II) M' = Cadmium(II), Zinc(II). These complexes were reacted...

DOI: 10.33899/rjs.2019.159987

Pages: 228-234